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用流动注射氢化物原子吸收法测定土壤中的砷和沉积物中的汞

赵兴敏 董德明 王文涛 花修艺

吉林大学学报(理学版)2009,Vol.47Issue(6):1303-1308,6.
吉林大学学报(理学版)2009,Vol.47Issue(6):1303-1308,6.

用流动注射氢化物原子吸收法测定土壤中的砷和沉积物中的汞

Determination of Arsenic in Soil and Mercury in Sediment by Flow Injection Hydride Atomic Absorption Spectrometry

赵兴敏 1董德明 2王文涛 1花修艺1

作者信息

  • 1. 吉林大学,环境与资源学院,长春,130012
  • 2. 吉林农业大学,资源与环境学院,长春,130118
  • 折叠

摘要

Abstract

As in soil and Hg in sediment were determined by flow injection hydride atomic absorption spectrometry. Under the optimum conditions of sample digestion and instrumental performance, the determining method is sensitive and accurate. For the determination of arsenic in soil, the limit of detection was found to be 2 ng/L and the recovery was in a range of 93. 6% ~ 106. 1% , RSDs were in a range of 1.36% ~ 5.08%. For determination of mercury in the sediment, the limit of detection was found to be 3 ng/L and the recovery was in a range of 93.2% ~ 109.6% , RSDs were in a range of 0.97% ~ 5. 53%. The flow injection hydride atomic absorption spectrometry has a high sensitivity and stability in determining arsenic in soil and mercury in sediment and its precision and accuracy are up to the standard of analysis.

关键词

流动注射氢化物原子吸收法/土壤//沉积物/

Key words

flow injection hydride atomic absorption spectrometry/ soil/ arsenic/ sediment/ mercury

分类

化学化工

引用本文复制引用

赵兴敏,董德明,王文涛,花修艺..用流动注射氢化物原子吸收法测定土壤中的砷和沉积物中的汞[J].吉林大学学报(理学版),2009,47(6):1303-1308,6.

基金项目

国家重点基础研究发展计划973项目基金(批准号: 2004CB418505). (批准号: 2004CB418505)

吉林大学学报(理学版)

OA北大核心CSCDCSTPCD

1671-5489

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