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均相共沉淀法制备氧化锌基红色荧光粉

胡文远 刘勋 杨定明 魏贤华

人工晶体学报2009,Vol.38Issue(5):1211-1215,5.
人工晶体学报2009,Vol.38Issue(5):1211-1215,5.

均相共沉淀法制备氧化锌基红色荧光粉

Preparation of ZnO Nano-phosphor Powders by Homogeneous Co-precipitation Method

胡文远 1刘勋 1杨定明 1魏贤华1

作者信息

  • 1. 西南科技大学材料科学与工程学院,绵阳,621010
  • 折叠

摘要

Abstract

The nano-phosphor powders of Eu, Li co-doped ZnO were prepared by homogeneous co-precipitation and thermal decomposition method using Zn(NO_3)_2·2H_2O,CO(NH_2)_2,Eu(NO_3)_3·6H_2O and LiNO_3·2H_2O as raw materials. The characteristics of samples were investigated by means of TG-DSC, XRD, SEM, FL. The results showed that the samples exhibited normal size distribution, whose size was about 20~40 nm. The photoluminescence intensity of samples was interrelated with thermal decomposition temperature, ratio of Li and Eu. The maximum emission spectra peak of samples was at λ_(em)=611 nm with 463 nm excitation, corresponding to ~5D_0→~7F_2 transition of Eu.

关键词

均相共沉淀/ZnO/纳米/荧光

Key words

homogeneous co-precipitation/ ZnO/ nanopowders/ photo luminescence

分类

数理科学

引用本文复制引用

胡文远,刘勋,杨定明,魏贤华..均相共沉淀法制备氧化锌基红色荧光粉[J].人工晶体学报,2009,38(5):1211-1215,5.

基金项目

国家自然科学基金(No.50802078) (No.50802078)

西南科技大学青年预研基金项目(06ZX3129) (06ZX3129)

人工晶体学报

OA北大核心CSCDCSTPCD

1000-985X

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