山西大学学报（自然科学版）2009，Vol.32Issue(4)：592-595,4.
微波辅助合成蒽醌类衍生物方法研究
Synthesis Process of Anthraquinone Derivatives Under Microwave Irradiation
摘要
Abstract
A rapid, facile and effective method for the preparation of anthraquinone derivatives was reported in this article. The anthraquinone derivatives were synthesized from the reaction of aromatic compounds with phthalic anhydride in the presence of AlCl_3/PPA or AlCl_3/H_2SO_4 as a catalyst under microwave heat-ing. In addition,the effects of different types of catalysts on the reaction yield were investigated. The re-suits indicated that AlCl_3/H_2SO_4 was a good catalyst for the synthesis of anthraquinone derivatives with e-lectron donating group. Whereas, AlCl_3/PPA was a good catalyst for substituted benzenes with electron withdrawing groups. These compounds have been characterized by UV, IR,~1H NMR and MS.关键词
蒽醌/微波辐射/一步合成法Key words
anthraquinone/microwave heating/one-pot synthesis分类
化学化工引用本文复制引用
张立伟,苏强,冯丽恒..微波辅助合成蒽醌类衍生物方法研究[J].山西大学学报（自然科学版）,2009,32(4):592-595,4.基金项目
国家自然科学基金(20802042) （20802042）
