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微波消解-氢化物原子荧光光谱法测定粤东地区海产品中砷的研究

蔡龙飞 徐春秀 张应钦 邱新红

安徽农业科学2011,Vol.39Issue(18):10985,10994,2.
安徽农业科学2011,Vol.39Issue(18):10985,10994,2.

微波消解-氢化物原子荧光光谱法测定粤东地区海产品中砷的研究

Determination of Arsenic in Seafood by Hydride Generation-atomic Fluorescence Spectrometry Combined with Microwave Oven Digestion

蔡龙飞 1徐春秀 1张应钦 1邱新红1

作者信息

  • 1. 韩山师范学院化学系,广东,潮州,521041
  • 折叠

摘要

Abstract

[Objective] The aim was to establish an effective determination method of arsenic in seafood. [Method] Contents of arsenic in seafood samples from eastern Guangdong area were determined by hydride generation-atomic fluorescence spectrometry combined with microwave oven digestion. [Result] The linear range for detection of arsenic was 1.0- 50.0 μg/L, which showed a good linear relationship,and its correlation coefficient was 0.995. The detection limit and relative standard deviation were 0.021 07 μg/L and 0.932% .respectively. Contents of arsenic in some seafood samples were more than the national standard,which could be caused by industrial pollution in coastal areas. [Conclusion] The method is simple,rapid and accurate,so it is applied to the determination of arsenic in seafood samples.

关键词

微波消解/原子荧光光谱法/海产品//测定

Key words

Microwave digestion/ Atomic fluorescence spectrometry/ Seafood/ Arsenic/ Determination

分类

农业科技

引用本文复制引用

蔡龙飞,徐春秀,张应钦,邱新红..微波消解-氢化物原子荧光光谱法测定粤东地区海产品中砷的研究[J].安徽农业科学,2011,39(18):10985,10994,2.

基金项目

韩山师范学院青年科学基金项目(413611,413615). (413611,413615)

安徽农业科学

0517-6611

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