安徽农业科学2011,Vol.39Issue(18):10919-10921,3.
2-(2-呋喃基)苯并咪唑及其钴、镍配合物的合成
Syntheses of Fuberidazole add Corresponding Co(Ⅱ),Ni(Ⅱ)Complexes
摘要
Abstract
The experimental process to synthesize fuberidazole by O-phenylendiamine with furfural was studied,and the influence of molar ratio of raw materials and the amount of HCl on product yield was discussed. On above basis,an optimal synthesis strategy and the purified method were put forwarded. Under the optimum conditions,the best yield reached 90.7%. Besides,Co(Ⅱ) ,Ni(Ⅱ) complexes incorporated with fuberidazole were synthesized and determined with EA,IR,NMR.关键词
2-(2-呋喃基)苯并咪唑/合成方法优化/钴、镍配合物Key words
Fuberidazole/ Optimal synthesis strategy/ Co(Ⅱ) ,Ni(Ⅱ) complexes分类
农业科技引用本文复制引用
苏碧云,郭晚雪,王建民..2-(2-呋喃基)苯并咪唑及其钴、镍配合物的合成[J].安徽农业科学,2011,39(18):10919-10921,3.基金项目
陕西省自然科学基础研究计划项目(2009JQ2006) (2009JQ2006)
陕西省教育厅专项科研计划项目(09JK696). (09JK696)