湖南中医药大学学报2011,Vol.31Issue(7):29-31,37,4.DOI:10.3969/j.issn.1674-070X.2011.07.008.029.03
通宣益气丸的质量标准研究
Study on quality standard of Tongxuan Yiqi pills
王青 1蔡萍 2万丹2 2陈秋香33
作者信息
- 1. 湖南中医药大学第二附属医院,湖南长沙410005
- 2. 湖南省中医药研究院,湖南长沙410006
- 3. 长沙市中医院,湖南长沙410010
- 折叠
摘要
Abstract
Objective To set up a quality standard of Tongxuan Yiqi pills. Methods Hhe TLC method was used for identifying Flos Lonicerae Japonicae, Radix Paeoniae Rubra and Radix Astragali. The content of Baicali was determined by HPLC. Results Flos Lonicerae Japonicae, Radix Paeoniae Rubra and Radix Astragali could be detected with TLC without any disturbing; the baicalin was detected with HPLC in a good linear relation within the range of 0.14-0.84 μg, r=0.999 6, the average recovery rate was 96.83% and RSD was 1.75%. Conclusion The method is suitable for the quality control of Tongxuan Yiqi pills.关键词
通宣益气丸/薄层色谱法/高效液相色谱法/黄芩苷/质量标准Key words
Tongxuan Yiqi pills/TLC/HPLC/Baicali/quality standard分类
医药卫生引用本文复制引用
王青,蔡萍,万丹2,陈秋香3..通宣益气丸的质量标准研究[J].湖南中医药大学学报,2011,31(7):29-31,37,4.