现代科学仪器Issue(3)：97-99,3.
GC-MS法分析蔬菜、水果、食用菌中嘧霉胺等4种农药残留及基质效应探讨
Determination of 4 Pesticides Residues Included Pyrimethanil in Vegetables, Fruits and Edible Mushrooms by GC/MS and Discussion of Matrix Effects
易盛国 1侯雪 1杨晓凤 1韩梅1
作者信息
- 1. 四川省农业科学院分析测试中心,四川成都610066
- 折叠
摘要
Abstract
A method based on GC/MS was developed to detect 4 pesticides residues included pyrimethanil, fipronil, pyridaben and difenoconazole in vegetables, fruits and edible mushrooms. Pesticides were extracted with acetonitrile, were cleaned up by an NH2/CARB0N SPE column, were separated on a capillary column (HP-5MS, 30 m*0.25 mm><0.25 um), then were determined with GC/MS/SIM and were quantified by extend method of matrix-matched calibration standard. The recoveries of 4 pesticides were in the range of 87.2%~108.7% with RSD (n=5) of 2.2%~6.9% at the spiked level of 0.10 mg/kg, and the limit of detection were 2.6 ug/kg~14.9 ug/kg. This method is suitable for the detection of multi-pesticide residues in vegetable, fruit and edible mushroom.关键词
GC-MS/农药残留/基质效应Key words
GC/MS/ Pesticides residues/ Matrix effects分类
化学化工引用本文复制引用
易盛国,侯雪,杨晓凤,韩梅..GC-MS法分析蔬菜、水果、食用菌中嘧霉胺等4种农药残留及基质效应探讨[J].现代科学仪器,2011,(3):97-99,3.
