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玄武岩玻璃的电子探针分析

孙志华 刘开平 刘民武

岩矿测试2011,Vol.30Issue(4):446-450,5.
岩矿测试2011,Vol.30Issue(4):446-450,5.

玄武岩玻璃的电子探针分析

Analysis of Basalt Glass by Electron Probe Micro Analyzer

孙志华 1刘开平 2刘民武3

作者信息

  • 1. 长安大学材料科学与工程学院,陕西西安710054
  • 2. 长安大学西部矿产资源与地质工程教育部重点实验室,陕西西安710054
  • 3. 西安交通大学电子材料研究所,陕西西安710049
  • 折叠

摘要

Abstract

This method analyzes the components of SiO2, CaO, A12O3, Fe2O3, MgO, K2O, TiO2, Na2O and P2O5 of basalt glass by JEOL JXA-8100 electron probe micro-analyzers. In order to accurately determine the contents of silicate quickly, the various analysis conditions were optimized for different analysis purposes, such as prismatic crystal, probing spot, accelerating voltage, revised means, beam current and so on. The optimum conditions were utilized to determine the components of silicate by comparing experimental data. The results show that small prismatic crystals of high sensitivity should be selected for low contents element measurements and the characteristic wavelength of the determined elements should be chosen in the mid wave band of the testing range. Accuracy can be improved by increasing accelerating voltage and beam current for low content samples. A larger probing spot should be selected for the elements which mobile easily. The PRZ method was applied to correct data of the multi-elements samples, which carry a large range of atomic numbers.

关键词

玄武岩玻璃/电子探针/硅酸盐

Key words

basalt glass/ electron probe micro-analyzers/ silicate

引用本文复制引用

孙志华,刘开平,刘民武..玄武岩玻璃的电子探针分析[J].岩矿测试,2011,30(4):446-450,5.

基金项目

西部交通建设科技项目(200831881263) (200831881263)

中央高校基本科研业务费专项基金(CHD2010JC076) (CHD2010JC076)

长安大学基础研究支持计划专项基金 ()

岩矿测试

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