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等离子光谱法测定岩石中微量元素的不确定度评定

杨红晓 张林群 周爱东

南京师大学报(自然科学版)2011,Vol.34Issue(3):69-73,5.
南京师大学报(自然科学版)2011,Vol.34Issue(3):69-73,5.

等离子光谱法测定岩石中微量元素的不确定度评定

Uncertainty Evaluation for Determination of Trace Elements in Rock by Inductively Coupled Plasma Atomic Emission Spectrometry

杨红晓 1张林群 1周爱东2

作者信息

  • 1. 南京师范大学分析测试中心,江苏,南京,210046
  • 2. 南京大学化学化工学院,江苏,南京,210093
  • 折叠

摘要

Abstract

The sources for the uncertainty were analyzed in detail for the determination ot trace elements including copper, zinc, plumbum, manganese, nickel, and chromium in rock by inductively coupled plasma atomic emission spectro-metric method. The main sources of measurement uncertainty come from sub-uncertainties of the analytical balance, analytical glassware, calibration curves, calibration solutions, reagent volume and repetitive measurements. Each sub - uncertainty, combined uncertainty and expanded uncertainty of the measurement results were calculated, and the report form of testing result was obtained.

关键词

不确定度评定/等离子体发射光谱法/微量元素/岩石

Key words

uncertainty evaluation/inductively coupled plasma atomic emission spectrometry (ICP-AES) /trace elements/rock

分类

化学化工

引用本文复制引用

杨红晓,张林群,周爱东..等离子光谱法测定岩石中微量元素的不确定度评定[J].南京师大学报(自然科学版),2011,34(3):69-73,5.

基金项目

国家自然科学基金面上预研资助项目(1116020501). (1116020501)

南京师大学报(自然科学版)

OA北大核心CSCDCSTPCD

1001-4616

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