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粉条加工中添加石蜡的检测技术研究

袁秀金 赵天珍

南方农业学报2011,Vol.42Issue(8):972-974,3.
南方农业学报2011,Vol.42Issue(8):972-974,3.

粉条加工中添加石蜡的检测技术研究

Development of a method to detect paraffin added during the processing of vermicelli

袁秀金 1赵天珍1

作者信息

  • 1. 中山市质量计量监督检测所,广东中山528403
  • 折叠

摘要

Abstract

[Objective]The present study was carried out to determine the paraffin contents added during vermicelli processing to help in food quality supervision in order to maintain food safety standards. [ Method ]The suitable conditions for detection of paraffin were optimized using gas chromatography-mass spectrometry (GC-MS) and an experiment with Cl8H38 and C24H50 was performed to test recovery rate and relative standard deviations. [ Result )The recovery rate of C18H38 and C24H50 were the highest (93.5 and 91.0%, respectively) in vermicelli treated with ultrasonic extraction method. Ultrasound time of 20 min was suitable for extracting alkane components in vermicelli. The relative standard deviations for developed detection method ranged from 3.6-4.8%, and the recovery rate was over 90%, which has achieved the quantitative requirement. [Conclusion]The developed method was found suitable for determination of paraffin content in vermicelli during its processing, qualitatively as well as quantitatively.

关键词

粉条/石蜡检测/回收率/检出限

Key words

paraffin/ vermicelli/ recovery rate/ detection limit

分类

轻工纺织

引用本文复制引用

袁秀金,赵天珍..粉条加工中添加石蜡的检测技术研究[J].南方农业学报,2011,42(8):972-974,3.

基金项目

广东省质量技术监督局科技资助项目(2009zz11) (2009zz11)

南方农业学报

OA北大核心CSCDCSTPCD

2095-1191

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