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大孔吸附树脂法提取急性子总皂苷的方法

李绪文 孟磊 李清民 佟亚楠 金永日 陈伟

吉林大学学报(理学版)2011,Vol.49Issue(5):949-953,5.
吉林大学学报(理学版)2011,Vol.49Issue(5):949-953,5.

大孔吸附树脂法提取急性子总皂苷的方法

Method of Total Hosenkosides Extraction from the Seeds of Impatiens balsamina L.with Macroporous Adsorption Resin

李绪文 1孟磊 1李清民 1佟亚楠 1金永日 1陈伟2

作者信息

  • 1. 吉林大学化学学院,长春130012
  • 2. 吉林大学中日联谊医院,长春130031
  • 折叠

摘要

Abstract

Four kinds of main hosenkosides named as hosenkosides K, A, C,B were used as the indexes of total hosenkosides extracted from the seeds of Impatiens balsamina L. The effects of the density, pH and the rate of the flow of the solution on the adsorption properties of the resin were investigated through the orthogonal test, establishing the adsorption conditions. The results show that the solutions were combined after filtration and evaporated to the 6 times the material weight in vacuum. The solution at pH 6.0 was passed through the AB-8 macroporous resin at a flow rate of 3 volumes of the resin in 1 h, then eluted by 80% ethanol. This way could collect the total hosenkosides, in which the content of the sum of four hosenkosides K, A, C, B was in the highest point.

关键词

急性子/总皂苷/大孔树脂/正交试验

Key words

Impatiens balsamina L. / total hosenkoside/ macroporous resin/ orthogonal test

分类

化学化工

引用本文复制引用

李绪文,孟磊,李清民,佟亚楠,金永日,陈伟..大孔吸附树脂法提取急性子总皂苷的方法[J].吉林大学学报(理学版),2011,49(5):949-953,5.

基金项目

国家科技支撑计划项目(批准号:2007 BA138B05). (批准号:2007 BA138B05)

吉林大学学报(理学版)

OA北大核心CSCDCSTPCD

1671-5489

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