中国药业2011,Vol.20Issue(24):49-51,3.
黄虎胶囊质量标准研究
Study on Quality Standards of Huanghu Capsule
冯建安 1谢守德 1李希 1易晓霞 2唐晓莹2
作者信息
- 1. 四川省中医药科学院中医研究所,四川,成都,610031
- 2. 成都中医药大学药学院,四川,成都,610075
- 折叠
摘要
Abstract
Objective To establish the quality standards of Huanghu Capsule. Methods Rhizoma polygoni cuspidati, Rhizoma coptidis, Radix sophorae tonkinensis, herba gentianae cephalanthae were identified by thin layer chromatography (TLC).The content of emodin was determined by HPLC. Results The spots of TLC were distinct and well separated. The negative sample had no interference. The linear regression for emodin was obtained over the range of 21. 84 - 109. 20 μg/mL( r =0. 999 9). The average recovery rate was 99.32%, RSD = 1.87% (n = 6). Conclusion The established methods can be used for the identification and quantification of the preparation.关键词
黄虎胶囊/质量标准/薄层色谱法/高效液相色谱法/大黄素Key words
Huanghu Capsule/ quality standards/ TLC/ HPLC/ emodin分类
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冯建安,谢守德,李希,易晓霞,唐晓莹..黄虎胶囊质量标准研究[J].中国药业,2011,20(24):49-51,3.