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烟草中氯的AAⅢ连续流动分析仪测定改进

王颖 张威 王洪波 刘惠民 唐纲岭 胡清源 范国民

烟草科技Issue(9):41-44,4.
烟草科技Issue(9):41-44,4.

烟草中氯的AAⅢ连续流动分析仪测定改进

Modification of AA Ⅲ Autoanalyzer Used for Determining Chloride in Tobacco

王颖 1张威 1王洪波 2刘惠民 2唐纲岭 1胡清源 1范国民3

作者信息

  • 1. 国家烟草质量监督检验中心,郑州高新技术产业开发区枫杨街2号 450001
  • 2. 中国烟草总公司郑州烟草研究院,郑州高新技术产业开发区枫杨街2号 450001
  • 3. 河南中烟工业有限责任公司驻马店卷烟厂,河南省驻马店市金桥开发区南区翠柏路6号 463000
  • 折叠

摘要

Abstract

In order to reduce the deviation in determining chloride in tobacco by A A DI autoanalyzer, the effects of dialyzer, wavelength for detection sample injection rate and color developing reagent concentration on the determination results were investigated, and the autoanalyzer was modified. The results showed that; 1) Tobacco extract could be purified by adding a dialyzer at reaction pipe. 2) Max adsorbance of reaction product was at the wavelength of 460 nm. 3) After modification, the recovery of the method were from 94.2% to 106.5% with RSD <5 %o The modified AA HI autoanalyzer is suitable for the accurate determination of chloride in tobacco.

关键词

AAⅢ连续流动分析仪/烟草/

Key words

AADI autoanalyzer/ Tobacco/ Chloride

分类

轻工纺织

引用本文复制引用

王颖,张威,王洪波,刘惠民,唐纲岭,胡清源,范国民..烟草中氯的AAⅢ连续流动分析仪测定改进[J].烟草科技,2011,(9):41-44,4.

基金项目

国家烟草专卖局标准项目"烟草及烟草制品氯的测定-连续流动法"(2009B0150). (2009B0150)

烟草科技

OA北大核心CSTPCD

1002-0861

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