医药导报2012，Vol.31Issue(1)：75-76,2.DOI:10.3870/yydb.2012.01.029
气相色谱法测定小金胶囊中麝香酮的含量
Content Determination of Muscone in Xiaojin Capsules by Gas Chromatography
卢敏 1胡振波 1王颖峰 1向阳1
作者信息
- 1. 武汉健民药业集团股份有限公司,430052
- 折叠
摘要
Abstract
Objective To establish a method for content determination of muscone in xiaojin capsules. Methods AT. OV-1301 column ( 30 m×0. 25 mm ,0. 25 μm ) was applied, the initial temperature of oven was set at 200℃ for 10 minutes, then it was raised to 250 ℃ for 10 minutes at rate of 30 ℃per minute. The temperature of injection port was 200℃. The detector was FID, which was at 280 ℃. Results The calibration curves were linear in the range of 46-736 ng for muscone( r = 0. 999 8 ). The average recovery was 100. 10%( RSD= 1. 61% ). Conclusion The method is simple, rapid, accurate, which can be used for the quality control of xiaojin capsules.关键词
小金胶囊/麝香酮/含量测定/色谱法,气相Key words
Xiaojin capsules/Muscone/Content determination/Gas chromatography分类
医药卫生引用本文复制引用
卢敏,胡振波,王颖峰,向阳..气相色谱法测定小金胶囊中麝香酮的含量[J].医药导报,2012,31(1):75-76,2.
