西安工程大学学报2011，Vol.25Issue(5)：684-688,5.
一种新型芳香酰腙的合成与结构表征
Synthesis and structure characterization of a new aromatic hydrazone
唐小冬 1郑长征 1田晓雪1
作者信息
- 1. 西安工程大学环境与化学工程学院,陕西西安710048
- 折叠
摘要
Abstract
The title compound of l-(4-methoxyphenyl) ethanone 4-chlorob-en2oyl hydrazone was synthesized by the reaction of 4-methoxyphenyl ethyl ketone and 4-chlorobenzoyl hydrazine. The structure of the compound was characterized by elemental analysis and X-ray diffraction. It was assigned to orthorhombic crystal sy-stem, space group Pca2(l),cell data:a=0. 850 7(5)nm,a =90°,6 =0.557 1 (3)nm,￡ = 90°, c = 3.215 4(18)nm,y = 90°,V = 1.523 9(14)nm3,Z=4,F(000) =632,/?, =0.031 7 [/ >2sigma(/)] ,wR2 =0.089 6. CCDC is 826 435.关键词
酰腙/晶体结构/X射线衍射Key words
hydrazone/crystal structure/X-ray diffraction分类
化学化工引用本文复制引用
唐小冬,郑长征,田晓雪..一种新型芳香酰腙的合成与结构表征[J].西安工程大学学报,2011,25(5):684-688,5.
