安徽农业科学2011，Vol.39Issue(22)：13563-13564,13567,3.
液相色谱串联质谱检测动物源性食品中莫西丁克残留
Deter mination of Moxidection Residues in Animal-derived Food by LC-MS/MS
潘新明 1潘守奇 2于金玲 2张靖2
作者信息
- 1. 山东丽波日化股份有限公司,山东潍坊261031
- 2. 山东省潍坊出入境检验检疫局,山东潍坊261041
- 折叠
摘要
Abstract
[Objective]The research aimed to establish a detection method of moxidectin residues in the animal-derived food. [ Method]The sample purification method and test parameters were firstly optimized. Moxidection was extracted with acetonitrile and purified by dispersive solid-phase extraction( SPE). The content of moxidection in the animal-derived food was detected by LC-MS/MS. [ Result]The optimum mass spectrum conditions were as follows:ion source temperature of 300 ℃,spray needle pressure of 15 Psi,dry air current speed of 6 L/min. Under these conditions, the response value of son ion peak was highest. The detection limit of the method was 0.005 mg/kg,the recovery rate (n =6) was 81.08% - 113.72% in the range of 0.005 -0.02 mg/kg,with RSD of 4.21% -9.69%. [Conclusion]The method had simple steps,strong maneuverability, low dosage of organic solvent,low cost and less impurity disturbance,better precision and lower detection limit. So it was suitable for the rapid detection of moxidection in the animal-derived food.关键词
莫西丁克/液相色谱串联质谱/分散固相萃取Key words
Moxidectin/ LC-MS/MS/ Dispersive SPE分类
农业科技引用本文复制引用
潘新明,潘守奇,于金玲,张靖..液相色谱串联质谱检测动物源性食品中莫西丁克残留[J].安徽农业科学,2011,39(22):13563-13564,13567,3.
