现代农业科技Issue(18)：357-358,360,3.
固相萃取-高效液相色谱-荧光法测定食用菌中多菌灵的含量
Determination of Carbendazim in Edible Fungus by SPE-HPLC-FLD
张松成 1王小玲 1金锦长 1夏乐舜1
作者信息
- 1. 丽水出入境检验检疫局,浙江丽水323000
- 折叠
摘要
Abstract
A new method was established for the determination of carbendazim in edible fungus by solid phase extraction-high performance liquid chromatography with fluorescence detector（SPE-HPLC-FLD）. The edible fungus samples were extracted by ethyl acetate and purified by a solid phase extraction column. Then,the chromatographic separation was achieved on a ClS column. The mobile phase was 20 mmoL/L phosphate-aeetonitrile. The results showed that the recovery rates of carbendasim were between 85.5% to 95.4% with the relative standard deviations below 6.0%, and limit of quantification （LOQs）was 0.05 mg/kg. The method is simple,sensitive,accurate,and repeatable,and can be used for determination of carbendazim in edible fungus.关键词
食用茵/多茵灵/固相萃取/高效液相色谱/荧光检测/含量Key words
edible fungus/earbendasim/solid phase extraction/high performance liquid chromatography/fluorescence detection/content分类
化学化工引用本文复制引用
张松成,王小玲,金锦长,夏乐舜..固相萃取-高效液相色谱-荧光法测定食用菌中多菌灵的含量[J].现代农业科技,2011,(18):357-358,360,3.
