安徽农业科学2011，Vol.39Issue(34)：21348-21349,21471,3.
有机碱催化制备马来酸单淀粉酯的研究
Study on the Preparation of Maleic Acid Ester with Organic Base Catalyst
摘要
Abstract
[Objective] To prepare maleic acid ester with tapioca starch. [Method] Maleic acid ester was prepared after the tapioca starchwas activated, with maleic anhydride as agent, acetone as solvent, and pyridine as catalyst. The preparation conditions of maleic acid ester wereoptimized by single-factor test. [Result] The best preparation conditions of maleic acid ester were;lg activated tapioca starch,50 ℃ reactiontemperature, 1:3 molar ratio of activated slurch lo muleir anhydride, 1 ml pyridine and 7 h reaction time. [Conclusion] By adopting the bestpreparation conditions,the degree of substitution fur maleic acid ester was 0.332.关键词
活化淀粉/马来酸酐/有机碱/酯化淀粉/取代度Key words
Activated starch/ Maleic anhydride/ Organic base/ Esterification of starch/ Degree of substitution分类
化学化工引用本文复制引用
罗菊香,崔国星,张琳君,陈朝阳..有机碱催化制备马来酸单淀粉酯的研究[J].安徽农业科学,2011,39(34):21348-21349,21471,3.基金项目
福建省科技计划重大项目(2010H6020) （2010H6020）
福建省科技计划项目(JK2010059) （JK2010059）
高校服务海西建设重点项目(HX200803). （HX200803）
