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电感耦合等离子体质谱法测定松潘地产大黄药材中重金属元素

王珺 金琰琰 方成武 张明燕 马宗华 杨青山

安徽中医学院学报2012,Vol.31Issue(2):61-64,4.
安徽中医学院学报2012,Vol.31Issue(2):61-64,4.DOI:10.3969/j.issn.1000-2219.2012.02.020

电感耦合等离子体质谱法测定松潘地产大黄药材中重金属元素

Content Determination of Heavy Metal Elements in Rhubarb from Songpan County of Sichuan Province Using Inductively Coupled Plasma-Mass Spectra

王珺 1金琰琰 2方成武 1张明燕 1马宗华 1杨青山3

作者信息

  • 1. 安徽中医学院药学院,现代中药安徽省重点实验室,安徽,合肥,230031
  • 2. 安徽省食品药品检验所,安徽,合肥,230051
  • 3. 安徽中医学院科技处,安徽,合肥,230038
  • 折叠

摘要

Abstract

Objective To determine the contents of plumbum (Pb) , cadmium (Cd) , hydrargyri ( Hg) , cuprum (Cu) and arsenic (As) in thubarb from Songpan county of Sichuan province,in an attempt to evaluate the safety of thubarb based on whether or not the contents of heavy metal elements are out of limits.Methods Rhubarb samples were processed by microwave digestion (MVD). The contents of five heavy mental elements in thubarb from different areas and cultivations were detected by inductively coupled plasma-mass spectra (ICP-MS). Results The detection limits of five heavy metal elements ranged from 0. 02 to 0. 30 ng/ml. This method had good linear correlation for each element (r>0. 999 1). The contents of five heavy metal elements from 20 samples of thubarb were within the limits of national standards. Conclusion Based on the contents of heavy metal elements being within the limits,it can be concluded that thubarbs from Songpan county are safe for medicine,and Songpan area is suitable for the cultivation of thubarbs.

关键词

大黄/重金属元素/电感耦合等离子体质谱法/松潘

Key words

rhubarb/ heavy metal elements/inductively coupled plasma-mass spectra / Songpan

分类

中医学

引用本文复制引用

王珺 ,金琰琰,方成武,张明燕,马宗华,杨青山..电感耦合等离子体质谱法测定松潘地产大黄药材中重金属元素[J].安徽中医学院学报,2012,31(2):61-64,4.

基金项目

国家星火计划重点项目(2009GA710002) (2009GA710002)

安徽中医学院学报

OACSTPCD

2095-7246

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