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石墨包覆纳米镍颗粒的结构及磁性能的表征

罗宁 李晓杰 孙贵磊 王海涛

爆炸与冲击2011,Vol.31Issue(4):433-438,6.
爆炸与冲击2011,Vol.31Issue(4):433-438,6.

石墨包覆纳米镍颗粒的结构及磁性能的表征

Synthesis, morphology and magnetic properties of graphite-encapsulated nickel nanoparticles

罗宁 1李晓杰 1孙贵磊 2王海涛1

作者信息

  • 1. 大连理工大学工业装备结构分析国家重点实验室,辽宁大连116024
  • 2. 中国劳动关系学院安全工程系,北京100048
  • 折叠

摘要

Abstract

Aimed at synthesizing the encapsulation of nickel nanocrystal within graphitic carbon, effective experiments were carried out by adjusting the mole ratio of carbon source and metal source in these precursors. The chemical composition, nanostructures and magnetic properties of the composite particles were analyzed by using X-ray diffraction (XRD) , transmission electron microscopy (TEM), energy dispersive X-ray detector (EDX) and vibrating sample magnetometer (VSM). The results showed that the different size and spherical graphite-encapsulated nickel nanoparticles with a perfect core-shell structure had been prepared and that these magnetic composite particles mainly distributed in 10-55 nm. The magnetic measurements demonstrated that the as-prepared CENNPs took on super-paramagnetic or ferromagnetic behaviors at room temperature.

关键词

爆炸力学/石墨包覆镍/X射线衍射仪/复合纳米颗粒/磁性能

Key words

mechanics of explosion/ graphite-encapsulated nickel/ X-ray diffraction/ composite nanop-articles/ magnetic properties

分类

数理科学

引用本文复制引用

罗宁,李晓杰,孙贵磊,王海涛..石墨包覆纳米镍颗粒的结构及磁性能的表征[J].爆炸与冲击,2011,31(4):433-438,6.

基金项目

国家自然科学基金项目(10872044,10902023) (10872044,10902023)

辽宁省自然科学基金项目(2008161) (2008161)

爆炸与冲击

OA北大核心CSCDCSTPCD

1001-1455

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