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碳掺杂TiO2光催化剂的制备及其性能表征

潘青山 郑思宁 郑柳萍 颜桂炀

福建师范大学学报(自然科学版)2012,Vol.28Issue(1):73-76,92,5.
福建师范大学学报(自然科学版)2012,Vol.28Issue(1):73-76,92,5.

碳掺杂TiO2光催化剂的制备及其性能表征

Preparation and Characterization of Carbon-doped TiO2 Photocatalyst

潘青山 1郑思宁 1郑柳萍 1颜桂炀1

作者信息

  • 1. 福建师范大学化学与材料学院,福建福州350007
  • 折叠

摘要

Abstract

Glucose and tetrabutyl titanate were used as precursors, the photocatalyst C-TiO2 was successfully prepared by alcoholysis at room temperature. The effects of calcination temperature, catalyst dosage and initial pH of reaction solution were evaluated by the photocatalytic activity of degradation reactive brilliant red X-3B. The catalysts were characterized by X-ray diffraction (XRD) ,UV-Vis diffuse reflectance spectra (UV-Vis DRS) ,ther-mogravimetric analysis (TG-DTG) and scanning electron microscopy (SEM-EDS). The results showed that the C-doped TiO2 has the typical anatase structure and satisfied photo-catalytic efficiency on the degradation of reactive brilliant red X-3B under visible light. While the dosage of catalyst 1. 5 g · L-1, pH value 7~9> calcination temperature at 500 °C, visible light irradiation for two hours, the photocatalytic degradation of concentration is 100 mg · L-1 reactive brilliant red X-3B could reach above 70%.

关键词

醇解法/TiO2/碳掺杂/活性艳红X-3B/光催化

Key words

alcoholysis/ TiO2 carbon doping/ reactive brilliant red X-3B/ photocatalytic

分类

化学化工

引用本文复制引用

潘青山,郑思宁,郑柳萍,颜桂炀..碳掺杂TiO2光催化剂的制备及其性能表征[J].福建师范大学学报(自然科学版),2012,28(1):73-76,92,5.

基金项目

福州市科技局资助项目(CE0015) (CE0015)

宁德师范学院服务海西资助项目(2010H103) (2010H103)

福建师范大学学报(自然科学版)

OA北大核心CSCDCSTPCD

1000-5277

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