高等学校化学学报2011,Vol.32Issue(12):2721-2726,6.
预先负载原料法合成ZSM-5/SAPO-5复合分子筛
ZSM-5/SAPO-5 Composite Molecular SievesSynthesized by Preloading Raw Material Method
摘要
Abstract
ZSM-5 (core)/SAPO-5 ( shell) binary structure composite molecular sieves were synthesized by preloading raw material method. The effect of loading conditions on the formation and character of core/shell structure zeolite was investigated. These synthesized samples were characterized by XRD, SEM, EDS and FTIR, respectively. The results indicate that the pretreated condition affects the combination of phosphorus and ZSM-5, the crystallinity and particle morphology of composite significantly. Compared to hydrothermal synthesis method, this approach is helpful to forming smaller SAPO-5 particles and growing SAPO-5 on ZSM-5 surface under suitable pretreated condition.关键词
核壳双结构分子筛/ZSM-5分子筛/SAPO-5分子筛/负载原料法Key words
Core-shell binary structure zeolite/ ZSM-5 molecular sieve/ SAPO-5 molecular sieves/ Loading raw material method分类
化学化工引用本文复制引用
张强,李春义,山红红,杨朝合..预先负载原料法合成ZSM-5/SAPO-5复合分子筛[J].高等学校化学学报,2011,32(12):2721-2726,6.基金项目
山东省自然科学基金(批准号:ZR2009BQ018)资助. (批准号:ZR2009BQ018)