硅酸盐通报2011，Vol.30Issue(6)：1278-1281,4.
稀土离子掺杂Ba0.65Zr0.35F2.70上转换纳米晶的制备与表征
Preparation and Characterization of Rare Earth Doped Ba0.65 Zr0.35 F2.70 Up-conversion Nanocrystals
摘要
Abstract
Nanocrystalline up-conversion phosphor Ba0.65 Zr0.35 F2.70 : Er3+ , Yb3+ were prepared by hydrothermal method using EDTA as complexing agent. The phase transformation, structure and morphology of the sample were analyzed by XRD and TEM, and the grain size of the sample was 20-40 nm. The sample has most intense upconversion luminescence when the mole ratio of Yb3+: Er3+ is 4:1. The relationship between up-conversion relative intensity and pump power was also studied, and revealed that the luminescence peaks of 523 nm, 546 nm and it's 650 nm were all two-photon process.关键词
水热法/上转换/纳米晶/稀土掺杂Ba0.65 Zr0.35F2.70Key words
hydrothermal method/up-conversion/nanocrystal/rare earth doped Ba0.65Zr0.35F270分类
化学化工引用本文复制引用
王学荣,杨魁胜,王晶晶..稀土离子掺杂Ba0.65Zr0.35F2.70上转换纳米晶的制备与表征[J].硅酸盐通报,2011,30(6):1278-1281,4.基金项目
吉林省科技发展计划项目(No.20070515) （No.20070515）
长春市科技局科研计划项目(No.2009151) （No.2009151）
