广州化学2011，Vol.36Issue(3)：28-32,5.
阳离子改性壳聚糖的合成工艺
Synthesis of Modified Cationic Chitosan
摘要
Abstract
In the poor of alkaline conditions,the 2-hydroxypropyl trimethyl ammonium chloride group was introduced onto chitosan in order to obtain the cationic chitosan.Using orthogonal test,the optimal synthesis conditions was determined by measuring the degree of substitution of synthetic products,and products structures were characterized by infra-red spectrum.The results show that the optimal synthesis conditions were mCTS/mCTA=1∶5,the swelling time of 60 min,the alkalization temperature of 35℃,the reaction temperature of 60℃,the reaction time of 9 h.In these conditions the degree of substitution of synthetic products was about 88.8%,and the quatemary ammonium group is attached to the amino which is on the chtiosan.关键词
阳离子表面活性剂/壳聚糖/3-氯-2-羟丙基三甲基氯化铵/季铵盐Key words
cationic surfactant/chitosan/3-chloro-2-hydroxypropl trimethyl ammonium chloride/quaternary ammonium salt分类
化学化工引用本文复制引用
魏爱花,武朝军,牟占军,张海健..阳离子改性壳聚糖的合成工艺[J].广州化学,2011,36(3):28-32,5.基金项目
内蒙古工业大学科学研究项目 （）
