河北科技大学学报2011，Vol.32Issue(6)：615-616,634,3.
N-[2-(3,4-二甲氧基苯基)乙基-]-N'-(2-苯乙基)-1,6-己二酰胺合成新工艺
New synthesis technology of N-[2-(3,4-dimethoxyphenyl)ethyl]-N '-(2-phenylethyl)-1, 6-hexanediamide
摘要
Abstract
One new synthesis technology of N-[2(3,4-dimethoxyphenyl)ethyl]-N'-(2-phenylethyl)-1,6-hexanediamide was designed through chlorination, condensation, hydrolysis, chlorination and condensation reaction with hexanedioic acid monom-ethyl ester as raw material. The technology has the advantages of simple operation, easy separation and easy purification, while the yield of the compound is up to 75. 2%, and it is applicable to large-scale industrial production. The structure of the final product is characteried by 1 H NMR.关键词
已二酸单甲酯/N-[2-(3,4-二甲氧基苯基)乙基]-N’-(2-苯乙基)-1,6-己二酰胺/苯乙胺/3,4-二甲氧基苯乙胺/合成/表征Key words
hexanedioic acid monomethyl ester/ N-[2(3,4-dimethoxyphenyl)ethyl]-N'-(2-phenylethyl)-1,6-hexanediamide/benzenethanamine/3,4-dimethoxy- benzenethanamine s synthesis/characterization分类
化学化工引用本文复制引用
张宝华,史兰香..N-[2-(3,4-二甲氧基苯基)乙基-]-N'-(2-苯乙基)-1,6-己二酰胺合成新工艺[J].河北科技大学学报,2011,32(6):615-616,634,3.基金项目
河北省科技攻关项目(07215603D) （07215603D）
