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φ20mm离心萃取器的水力学性能

李传博 张宇 晏太红 郑卫芳 左臣 袁中伟

核化学与放射化学2011,Vol.33Issue(6):349-352,4.
核化学与放射化学2011,Vol.33Issue(6):349-352,4.

φ20mm离心萃取器的水力学性能

Hydraulic Performance of φ20 mm Centrifugal Extractor

李传博 1张宇 1晏太红 1郑卫芳 1左臣 1袁中伟1

作者信息

  • 1. 中国原子能科学研究院放射化学研究所,北京102413
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摘要

Abstract

In order to use ∮20 mm centrifugal extractors for experimental study of the 2A contactor of Purex process, the hydraulic properties of such a centrifugal extractor were investigated under the working conditions prescribed by the process parameters of the 2A contactor. By using 30% TBP/kerosene-HNO3 as the extraction system and fixing the heavy phase weir diameter to 10. 8 mm, the influence of aqueous-to-organic phase flow ratio (A : O), two-phase total flow rate, and rotation speed of the rotor on the entrainment of liquids from both light and heavy phase outlet, and on the volume of liquid in the mixing zone and that in the rotator were examined. The experimental results show that when the A:O is 1:1 and the total flow rate is less than 70. 0 mL/min, or the A : O is 5:1 and the total flow rate is less than 28. 8 mL/min, and the rotation speed is greater than 3 000 r/min, such type of centrifugal extractor works in a stable operational condition, liquids from both light and heavy phase outlet are not entrained. The liquid volume of the mixing zone is about 5. 1 mL, and the total liquid volume in the rotor is about 12. 3 mL. The two phase contact time is calculated to bet= 5.1×60/νt, where vt is the total flow rate. The results indicate that this type of centrifugal extractor can meet the requirements for process research of 2A contactor of Purex process.

关键词

离心萃取器/水力学性能/存留量

分类

能源科技

引用本文复制引用

李传博,张宇,晏太红,郑卫芳,左臣,袁中伟..φ20mm离心萃取器的水力学性能[J].核化学与放射化学,2011,33(6):349-352,4.

核化学与放射化学

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