火炸药学报2011,Vol.34Issue(6):88-90,3.
偏二甲肼苦味酸盐的合成与性能
Synthesis and Properties of Unsymmetrical Dimethylhydrazine(UDMH) Picrate
慕晓刚 1刘祥萱 1王煊军 1韩启龙 1李霞1
作者信息
摘要
Abstract
In order to solve the problem of reusing rejected unsymmetrical dimethylhydrazine(UDMH) ,a new compound named UDMH picrate was synthesized. Its molecular structure and thermal behavior were characterized by elemental analyses,FT IR,1H NMR,TG/DTG and DSC. The results showed that thermal decomposition of UDMH oxalate occurred over the temperature range from 175. 8°C to 244. 3°C and its melting point was about 152°C. The main thermal decomposition products of UDMH picrate obtained by TG-FTIR analysis were CO2 , H2O,NO2 ,N2O and NH3 etc.关键词
有机化学/偏二甲肼苦味酸盐/合成/表征Key words
organic chemistry/unsymmetrical dimethylhydrazine picrate/synthesis/characterization分类
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慕晓刚,刘祥萱,王煊军,韩启龙,李霞..偏二甲肼苦味酸盐的合成与性能[J].火炸药学报,2011,34(6):88-90,3.