日用化学品科学2011，Vol.34Issue(12)：16-18,3.
微波辐射下NaHSO_4·H_2O催化合成烷基糖苷
Synthesis of alkyl polyglucoside by NariSO4-H2O under microwave irradiation
周大鹏 1黄亚茹 1葛赞1
作者信息
- 1. 浙江赞宇科技股份有限公司,浙江杭州310009
- 折叠
摘要
Abstract
Alkyl polyglucoside was synthesized by direct reaction of glucose with laurel alcohol, with NariSO4 H2O as catalyst under microwave irradiation / ultrasonic irradiation. Influence of preparation conditions on conversion rate and product appearance were studied. The optimum conditions were obtained as following： microwave power of 300 W, radiation time of 30 min, ultrasonic power of 600 W, mole ratios n （aurel alcohol） ： n （glucose） = 5 ： 1, and w （catalyst） ： w （glucose）=1 ： 100. In this case, the conversion rate of glucose was up to 98.9% and the catalyst could be reused. IR spectrum of APG was analyzed.关键词
烷基糖苷/微波/超声波/催化Key words
alkyl polyglucoside/microwave/ultrasonic/catalyst分类
化学化工引用本文复制引用
周大鹏,黄亚茹,葛赞..微波辐射下NaHSO_4·H_2O催化合成烷基糖苷[J].日用化学品科学,2011,34(12):16-18,3.
