首都师范大学学报（自然科学版）2011，Vol.32Issue(5)：26-29,4.
钒配合物[ VO(Phen)2SO4]·4H2O·CH3CH2CHOHCH3的合成、晶体结构和谱学表征
Synthesis, Crystal Structure and Infrared Spectra of [VO(Phen)2 SO4 ] · 4H2 O· CH3 CH2 CHOHCH3
摘要
Abstract
[VO(Phen)2SO4]4H2O CH3CH2CHOHCH3 was sythesized at room temperature by solvothermal reation. The crystal structure of complex was determined by X - ray diffraction structure analysis and IR. The results show that complex belongs to monoclinic system with space group P21/c,a=11.842(4)nm,b=20.263(6)nm,c=12.794 (4) nm,β=91. 335(5), Z=4, R =0.0466(5 323), wR2 = 0.1613( 7030).关键词
1,10-邻菲哕啉/晶体结构/氢键作用Key words
phen/crystal structure/hydrogen bond分类
化学化工引用本文复制引用
朱琳丽,池子翔,鲁晓明..钒配合物[ VO(Phen)2SO4]·4H2O·CH3CH2CHOHCH3的合成、晶体结构和谱学表征[J].首都师范大学学报（自然科学版）,2011,32(5):26-29,4.
