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丙酮酸壳聚糖的合成及其吸附性能

梁婧宇 吕彤 韩冰

天津工业大学学报2011,Vol.30Issue(5):46-49,4.
天津工业大学学报2011,Vol.30Issue(5):46-49,4.

丙酮酸壳聚糖的合成及其吸附性能

Synthesis and adsorption properties of chitosan modified by pyruvic acid

梁婧宇 1吕彤 1韩冰1

作者信息

  • 1. 天津工业大学环境与化学工程学院,天津300387
  • 折叠

摘要

Abstract

Pyruvate ehitosam (PCTS) was successfully prepared from chitosan and pyruvic acid, after reductived by NaBH4. The structure of PCTS was determined by IR adsorption, field emission scanning electron microscopy and elements. The results show that the best synthesis condition is, the reaction time 4.5 h, pH 4.5, pyruvic acid with chitosan ami no mole ratio on 2:1 for the substitution degree 90.6%; 1.67 g/L PCTS adsorbed 30 mL 10 μg/ mL of the Pb2+ at pH 5.4 for 2 h, achieved adsorption equilibrium, the maximum adsorption is 27.1 mg/g, better than chitosan.

关键词

壳聚糖/丙酮酸/吸附性能

Key words

chitosan/ pyruvic acid/ adsorption properties

分类

化学化工

引用本文复制引用

梁婧宇,吕彤,韩冰..丙酮酸壳聚糖的合成及其吸附性能[J].天津工业大学学报,2011,30(5):46-49,4.

天津工业大学学报

OA北大核心CSTPCD

1671-024X

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