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Bi2WO6的水热合成及其光催化性能研究

刘瑛 王为民 傅正义 王皓 王玉成 张金咏

无机材料学报2011,Vol.26Issue(11):1169-1174,6.
无机材料学报2011,Vol.26Issue(11):1169-1174,6.DOI:10.3724/SP.J.1077.2011.01169

Bi2WO6的水热合成及其光催化性能研究

Hydrothermal Synthesis and Photocatalytic Properties of Bi2WO6

刘瑛 1王为民 1傅正义 1王皓 1王玉成 1张金咏1

作者信息

  • 1. 武汉理工大学材料复合新技术国家重点实验室,武汉430070
  • 折叠

摘要

Abstract

Series of bismuth tungstate (Bi2WO6) catalysts were synthesized through simple hydrothermal route and characterized by X-ray diffraction (XRD), field emission scanning electron microscope (FESEM) and UV-Vis diffuse reflectance spectroscope (DRS). The effects of synthesis conditions on the morphologies and properties of products were studied. UV-Vis diffuse reflectance spectra indicated that the samples had absorption in both UV and visible light areas. Their photocatalytic activities were determined by photodegradation of Rhodamine B (RhB) under UV and visible light irradiation (λ> 420 nm). The results indicated that sample reacted at 180°C for 24h (pH=2) had the best photocatalytic activities, with reaction rate constant k of 0.03688/min. The stability of photocatalysts was estimated, no obvious loss of photocatalytic property was detected after four cyclic tests. After 150min visible light irradiation, the degradation rate of dye to the Bi2WO6 reacted at 180°C for 24h (pH=2) reached 38%.

关键词

Bi2WO6粉体/水热合成/光催化性能/罗丹明B

Key words

Bi2WO6 powders/ hydrothermal synthesis/ photocatalytic properties/ rhodamine B (RhB)

分类

化学化工

引用本文复制引用

刘瑛,王为民,傅正义,王皓,王玉成,张金咏..Bi2WO6的水热合成及其光催化性能研究[J].无机材料学报,2011,26(11):1169-1174,6.

基金项目

国家自然科学基金(50821140308) (50821140308)

无机材料学报

OA北大核心CSCDCSTPCDSCI

1000-324X

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