| 注册
首页|期刊导航|现代科学仪器|离子色谱法测定食品中的硼酸盐

离子色谱法测定食品中的硼酸盐

邵宏宏 周向阳 周秀锦 徐君辉 傅谧妮

现代科学仪器Issue(4):50-52,3.
现代科学仪器Issue(4):50-52,3.

离子色谱法测定食品中的硼酸盐

Determination of Borate in Food by Ion Chromatography

邵宏宏 1周向阳 1周秀锦 1徐君辉 1傅谧妮1

作者信息

  • 1. 舟山出入境检验检疫局,浙江舟山316000
  • 折叠

摘要

Abstract

A method for the determination of borate in food by ion exclusion chromatography with suppressed conductivity was developed.Sample was injected by simple sample pretreatment.Chromatographic separation was performed on a Dionex IonPac ICE-Borate column,2.5mmol/L MSA+60mmol/L Mannitol eluent was used at a flow rate of 1.0 mL/min.The linear ranges of the method for borate was 0.025.00 μg/mL,the correlation coefficients were 0.9997,and the detection limits(S/N=3) of borate was 0.01 μg/mL.The method was successfully applied to determine borate in real samples.The recoveries of borate after spiking was between 85.0 % to 92.5 %.This method is rapid,simple and suitable for the determination of real samples

关键词

离子色谱/食品/硼酸盐

Key words

Ion chromatography/Food/Borate

分类

化学化工

引用本文复制引用

邵宏宏,周向阳,周秀锦,徐君辉,傅谧妮..离子色谱法测定食品中的硼酸盐[J].现代科学仪器,2011,(4):50-52,3.

基金项目

本文系浙江检验检疫局科技计划项目资助项目 ()

现代科学仪器

OACSTPCD

1003-8892

访问量3
|
下载量0
段落导航相关论文