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模板整理对SnO2/C遗态材料显微结构及性能的影响

贺辛亥 齐乐华 王俊勃 杨敏鸽 申明乾 畅巍

新型炭材料2011,Vol.26Issue(5):375-380,6.
新型炭材料2011,Vol.26Issue(5):375-380,6.

模板整理对SnO2/C遗态材料显微结构及性能的影响

Effect of biological template consolidation on the microstructure and properties of SnO2/C bio-morphic materials

贺辛亥 1齐乐华 2王俊勃 1杨敏鸽 2申明乾 2畅巍2

作者信息

  • 1. 西北工业大学机电学院,陕西西安710072
  • 2. 西安工程大学机电工程学院,陕西西安710048
  • 折叠

摘要

Abstract

Ramie fibers were treated by different finishing processes including water washing, NaOH soaking and oxidative bleaching. The three kinds of finished Ramie fibers as soft carbon precursor were chopped to 10-20 mm and blended with phenolic resin as hard carbon precursor with a weight ratio of fibers to resin of 1 :1 and 6mass% toluene sulfochloride as a hardening reagent. The blends were hot-pressed at 130℃ and carbonized at 800℃. The three carbon plates were repeatedly impregnated with Sn(OH)4 sol to a weight ratio of Sn(OH)4/ carbon of 0.5, followed by carbothermal reduction at 560℃ in vacuum to prepare SnO2/C bio-morphic materials. The effect of finishing processes on the phase composition and morphology of SnO2/C bio-morphic materials were analyzed by X-ray diffraction and scanning electron microscopy. In addition, the wear rates of the bio-morphic samples were tested using a home-made abrader. It was found that the microstructure and wear resistance of the SnO2/C bio-morphic materials are significantly different and could be effectively controlled through the finishing process.

关键词

生物模板/整理工艺/SnO2/C遗态材料/显微结构/磨损率

Key words

Bio-template/ Finishing process/ SnO2/C bio-morphic materials/ Microstructure/Wear rate

分类

通用工业技术

引用本文复制引用

贺辛亥,齐乐华,王俊勃,杨敏鸽,申明乾,畅巍..模板整理对SnO2/C遗态材料显微结构及性能的影响[J].新型炭材料,2011,26(5):375-380,6.

基金项目

陕西省科学技术研究发展计划项目(2011K07-10),陕西省教育厅自然科学专项基金(09JK449,2010JK579),中国纺织工业协会科技指导性项目(2008046),西安工程大学基础研究基金(XGJ08010). (2011K07-10)

新型炭材料

OA北大核心CSCDCSTPCDSCI

1007-8827

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