烟草科技Issue(10)：39-43,5.
微波消解-离子色谱法测定烟草中的全硫
Determination of Total Sulfur in Tobacco with Microwave Digestion-Ion Chromatography
郝红玲 1何爱民 1苏国岁1
作者信息
- 1. 河北中烟工业有限责任公司技术中心,石家庄市桥西区 050051
- 折叠
摘要
Abstract
In order to determine the content of total sulfur in tobacco with ion chromatography, the total sulfur in tobacco was converted into sulfate by microwave digestion treatment, and the digestion and acid removal conditions were investigated. The proposed method was validated by the analyses of national standard material, bush twigs and leaves, and the total sulfur and inorganic sulfur in some tobacco leaf samples were analyzed by this method and direct extraction-ion chromatography, respectively. The results showed that; 1) the recoveries of total sulfur ranged from 94. 8% to 101. 9% with the RSD of < 2% , the method demonstrated higher sensitivity, accuracy and repeatability; 2) the inorganic sulfur contents in the tested samples significantly positively correlated with total sulfur contents (r =0.9934).关键词
微波消解/离子色谱/烟草/全硫/无机硫Key words
Microwave digestion/ Ion chromatography/ Tobacco/ Total sulfur/ Inorganic sulfur分类
轻工纺织引用本文复制引用
郝红玲,何爱民,苏国岁..微波消解-离子色谱法测定烟草中的全硫[J].烟草科技,2011,(10):39-43,5.
