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油页岩灰渣制备纳米γ-Al2O3的方法研究

季桂娟 郝磊 李晓军 高桂梅 甘树才

中国非金属矿工业导刊Issue(3):29-30,53,3.
中国非金属矿工业导刊Issue(3):29-30,53,3.

油页岩灰渣制备纳米γ-Al2O3的方法研究

Method for Extracting Nano γ -Al2O3 by Oil Shale Ash

季桂娟 1郝磊 1李晓军 2高桂梅 1甘树才1

作者信息

  • 1. 吉林大学化学学院,吉林长春130026
  • 2. 大庆油田责任有限公司,吉林大庆163453
  • 折叠

摘要

Abstract

A combined process was proposed for the utilization of waste oil shale ash (OS A) in the production of y -A12O3 nanoparticles. The process consisted of two stages, leaching and sintering. The ultrasonic technique followed by a heterogeneous azeotropic distillation process in the presence of polyethylene glycol (PEG) was carried to ensure complete elimination of the residual water in the precipitate. The structural and morphological properties of the calcined nanocrystalline powders were characterized by X-ray diffractometer (XRD), transmission electron microscope (TEM), Brunauer-Emmett-Teller nitrogen-gas adsorption method (BET). The results indicated that the y -A12O3 powder with a uniform particle was well dispersed and the particle size was 20~40nm.

关键词

油页岩灰渣/共沸蒸馏/纳米γ -Al2O3

Key words

oil shale ash/ azeotropic distillation/ nano y -A12O3

分类

资源环境

引用本文复制引用

季桂娟,郝磊,李晓军,高桂梅,甘树才..油页岩灰渣制备纳米γ-Al2O3的方法研究[J].中国非金属矿工业导刊,2011,(3):29-30,53,3.

基金项目

国家重大科技专项课题资助(2008ZX05018-005). (2008ZX05018-005)

中国非金属矿工业导刊

OACSTPCD

1007-9386

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