中国畜牧兽医Issue(12)：119-121,3.
HPLC法检测猪肉中5种磺胺类药物残留的研究
Study on the Determination of Five Sulfonamides Residues in Pork with HPLC
杨静 1王世山 1刘树军 1成林 1张昕1
作者信息
- 1. 焦作市畜产品质量安全监测中心,河南焦作454000
- 折叠
摘要
Abstract
Five sulfonamides residues in pork were determined by HPLC. The influences of mobile phase, SPE column and elution rate on the experiment were discussed on the basis of Appendix E, NY5029-2001. Five sulfonamides residues could be separated efficiently when the proportion of methanol to acetonitrile to 2. 2% acetic acid solution was 15 ∶ 15∶ 70 with SB C18 column. Considerable recovery and experimental accuracy could be obtained when the Waters alumina B SPE column was employed and the elution rate was controlled.关键词
磺胺类药物残留/HPLC/固相萃取/回收率Key words
sulfonamides residues/HPLC/solid-phase extraction/recovery分类
农业科技引用本文复制引用
杨静,王世山,刘树军,成林,张昕..HPLC法检测猪肉中5种磺胺类药物残留的研究[J].中国畜牧兽医,2011,(12):119-121,3.
