中国药房2012，Vol.23Issue(3)：234-237,4.DOI:10.6039/j.issn.1001-0408.2012.03.16
山茱萸炮制前后的HPLC指纹图谱研究
Study on HPLC Fingerprints of Cornus officinalis before and after Processing
摘要
Abstract
OBJECTIVE: To establish HPLC fingerprints of crude and processed Cornus officinalis. METHODS: 14 batches of C. Officinalis hygiene products and 14 batches of processed products were selected from different origin at different acquisition time. Waters sunfire Cis(250 mmx4.6 mm, 5 urn) column was used with 0.1% phosphoric acid and methanol as mobile phase (gradient elution) at the flow rate of 0.8 mL ? Min"'. The column temperature was 30 T and detection wavelength was set at 240 run. RESULTS: 16 common peaks were detected in the chromatograms of C. Officinalis hygiene products, and 17 common peaks were detected in the chromatograms of C. Officinalis processed products. The chromatograms of different hygiene products were similar to those of processed products generally. They were separated well on the whole. CONCLUSION: On the whole, the characteristics of C. Officinalis hygiene products have been compared with processed products in the study. It provides effective methods for the quality control of C. Officinalis.关键词
山茱萸/高效液相色谱法/指纹图谱/炮制Key words
Cornus officinalis/ HPLC/ Fingerprints/ Processing分类
医药卫生引用本文复制引用
刘华亮,袁珂,陈年者,马征..山茱萸炮制前后的HPLC指纹图谱研究[J].中国药房,2012,23(3):234-237,4.基金项目
浙江省科技计划项目(2007C23024) （2007C23024）
