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楮头红化学成分的分离与鉴定

伏晓 樊建领 巨秦豫

中国药房2012,Vol.23Issue(7):638-639,2.
中国药房2012,Vol.23Issue(7):638-639,2.DOI:10.6039/j.issn.1001-0408.2012.07.22

楮头红化学成分的分离与鉴定

Isolation and Identification of Chemical Constituents from Sarcopyramis nepalensis

伏晓 1樊建领 1巨秦豫1

作者信息

  • 1. 河南省中医院药剂科,郑州 450002
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摘要

Abstract

OBJECTIVE: To isolate and identify chemical constituents from the ethanol extracts of Sarcopyramis nepalensis. METHODS: S. nepalensis were extracted with 60% ethanol. The ethanol extracts were successively partitioned with systematic solvent. The chloroform extract and ethyl acetate extract were separated by silica gel, Sephadex LH-20 and RP-ODS column. Their chemical structures were identified by physicochemical properties, NMR and ESI-MS spectral analysis. RESULTS: Seven chemical constituents were isolated and identified as β-Sitosterol (1),daucosterpl (2), kaempferol (3), quercetin (4),quercetin-3-0-β-D-glu-copyranoside (5), rutin (6) and kaempferol-3-O-β-D-glucopyranoside (7). Compounds 3~7 were isolated from the plant for the first time. CONCLUSION: The results provide the scientific basis for further exploitation of S. nepalensis.

关键词

楮头红/化学成分/分离/结构鉴定

Key words

Sarcopyramis nepalensis/ Chemical constituents/ Isolation/ Structure identification

分类

医药卫生

引用本文复制引用

伏晓,樊建领,巨秦豫..楮头红化学成分的分离与鉴定[J].中国药房,2012,23(7):638-639,2.

中国药房

OACSCDCSTPCD

1001-0408

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