中国药业2012，Vol.21Issue(5)：16-17,2.
原子荧光光谱法检测含铁包衣粉中铅含量
Research on Determination of Pb in Film Coating Powder with Iron by Atomic Fluorescence Spectrometry
邱湘龙 1张育胜 1赵艳红 1陈利明 1方卫卫1
作者信息
- 1. 温州小伦包衣技术有限公司,浙江温州,325011
- 折叠
摘要
Abstract
Objective To establish an atomic fluorescence spectrometric method for the determination of Pb in film coating powder with iron. Methods The sample was digested by the method of pressure digestion tank in the system of nitric acid - hydrogen peroxide, and then extracted by MIBK in 6-7mol/L hydrochloric acid to remove iron, and detected after being disposed. Results The recovery is 99.2% -101.5% and the RSD is 0. 81% ( ft = 6). Conclusion The method can effectively eliminate interference to determinate about iron and has better repeatability and recovery.关键词
原子荧光光谱法/包衣粉/铁/铅/干扰/甲基异丁基甲酮/萃取Key words
atomic fluorescence spectrometry/ film coating powder/ iron/ Pb/ interference/ MIBK/ extract分类
化学化工引用本文复制引用
邱湘龙,张育胜,赵艳红,陈利明,方卫卫..原子荧光光谱法检测含铁包衣粉中铅含量[J].中国药业,2012,21(5):16-17,2.
