中国中医药信息杂志2012,Vol.19Issue(1):60-62,3.DOI:10.3969/j.issn.1005-5304.2012.01.022
清瘟解毒分散片质量标准研究
Quality Standard of Qingwen Jiedu Dispersible Tablets
王晓莉 1刘成松1
作者信息
- 1. 甘肃中医学院附属医院,甘肃兰州730020
- 折叠
摘要
Abstract
Objective To establish the quality standard of Qingwen Jiedu Dispersible Tablets. Methods Radix scrophulariae, Fructus arctill and Radix puerariae in the formulation were identified by TLC. The content of baicalin was determined by HPLC with C18 column and using a mobile phase of MeOH-water-phosphonic acid (47 : 53 : 0.2) under the flow rate of 1.0 mL/min. The column temperature was 25 °C and the detection wavelength was 280 nm. Results The quanitative identification was specific. The linear range of the baicalin was 0.104-0.520 μg (r=0.999 8) and the average recovery rate was 98.72% (RSD=1.31%, n=5). Conclusion The eatablished standard is suitable for the quality control of Qingwen Jiedu Dispersible Tablets.关键词
清瘟解毒分散片/黄芩苷/薄层色谱法/高效液相色谱法/质量标准Key words
Qingwen Jiedu Dispersible Tablets/ baicalin/ TLC/ HPLC/ quality standard分类
医药卫生引用本文复制引用
王晓莉,刘成松..清瘟解毒分散片质量标准研究[J].中国中医药信息杂志,2012,19(1):60-62,3.