中药材2011，Vol.34Issue(12)：1841-1843,3.
GC-MS法对怀山药饮片中六种农药残留量的测定
Determination of 6 Kinds of Pesticides Residue in Dioscoreae Rhizoma Slices by GC-MS
蒋以号 1刘伟 2曹晖 1于留荣 1向飞军3
作者信息
- 1. 康美药业股份有限公司,广东普宁515341
- 2. 南昌大学环境与化学工程学院,江西南昌330031
- 3. 国家中药现代化工程技术研究中心,广东珠海519100
- 折叠
摘要
Abstract
Objective: To determine the 6 residues including organophosphorus, organochlorinated and pyrethroid pesticides simultaneously in crude yam slices,yam slices stir-fried with bran and sulfur fumigation yam. Methods: The compounds were ready for GCMS analysis after being extracted with acetonitrile and purified. Determinations were performed with selected ion monitoring mode and external standard method was adopted in the quantificaticon . Results: The contents of 6 kinds pesticides residue had good linear correlation with the peak area in the rang of 0. 01 ~0. 5μg/mL. The average recoveries of 6 kinds pesticides residue were 87. 5 % -95. 5%. The method detection limits ranged from 0. 002 ~ 0. 005 μg/g. Organochlorine and pyrethroid pesticides were detected in the three samples except the parathion residue. Conclusion: Stir-fried with bran and sulphur fumigation had nearly no effects on the pesticides residue in yam. The method is sensitive and accurate and can be used in determination of multiresidual pesticides residue in yam.关键词
山药饮片/农药/残留/气质联用法Key words
Processed yam/Pesticides/Residues/GC-MS分类
医药卫生引用本文复制引用
蒋以号,刘伟,曹晖,于留荣,向飞军..GC-MS法对怀山药饮片中六种农药残留量的测定[J].中药材,2011,34(12):1841-1843,3.
