广西植物2012,Vol.32Issue(2):261-263,3.DOI:10.3969/j.issn.1000-3142.2012.02.023
马兰化学成分研究 (Ⅱ)
Studies on the chemical constituents of Kalimeris indica(Ⅱ)
摘要
Abstract
The chemical constituents were extracted from Kalimerisindica by cold percolation extraction . Compounds were isolated and purified with silica gel and Sephadex LH-20 column chromatography, the structures were deter mined on the basis of physicochemical evidence and ectroscopic analysis. Twelve compounds were separated and puri fied from water insoluble parts of 80% alcohol extracts of K. Indica. They were identified as n-Hexadecanioc acid (l),6-Hydroxy-eudesm-4(14)-ene(2),p-Sitosterol(3),crSpinasterol(4),Vanillin(5),3-Oxo-dammara-20(21) ,24 dene(6),Stigmasterol(7),Friedelin(8) 、Iupeone(9),a-Amyrin(10),Friedel-3-ol(ll),(2S,3S,4R,8E)-2-[(2R')-2' Hydroxyteracosenoilamino]-8-octadecene-l,3,4-triol(12). Compounds 2,6,9,12 were isolated from this plant for the first time.关键词
马兰/渗漉提取/分离鉴定/化学成分Key words
Kalimeris indica/ percolation process/ isolation and structure identification/ chemical constituents分类
农业科技引用本文复制引用
钟文武,刘劲松,张聪佴,陈爱民,许应生,王刚..马兰化学成分研究 (Ⅱ)[J].广西植物,2012,32(2):261-263,3.基金项目
安徽省自然科学基金(11040606W220) (11040606W220)
康缘中医药科技创新基金(KYCX 201003) (KYCX 201003)