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煅烧制度对Lu2Ti2O7粉体生长形貌的影响

李宝让 高慧 张乃强 徐鸿

人工晶体学报2012,Vol.41Issue(1):146-151,6.
人工晶体学报2012,Vol.41Issue(1):146-151,6.

煅烧制度对Lu2Ti2O7粉体生长形貌的影响

Influences of Calcining Process on Lu2Ti2O7 Powder Morphology

李宝让 1高慧 1张乃强 1徐鸿1

作者信息

  • 1. 华北电力大学电站设备状态监测与控制教育部重点实验室,北京 102206
  • 折叠

摘要

Abstract

Lu2Ti2O7 powders were prepared by molten salt synthesis process. The effect of calcining process on morphology of Lu2Ti2O7 powder was investigated. The efficient processes were determined. Lu2Ti2O7 powders were characterized by XRD and SEM. Based on these experimental results, a preliminary growth mechanism of time-dependent particle evolution was given. The studies revealed the nucleation and growth rate played important roles in determining the geometric shape and size of the product. High nucleation and particle growth rate easily made the agglomerated crystals convert into hexahedral prismatic form while the smaller nucleation and growth rate allowed the particles to have good crystallinity and regular polyhedral crystal faces.

关键词

Lu2Ti2O7/熔盐法/生长机制

Key words

Lu2Ti2O7 powders/molten salt synthesis/growth mechanism

分类

矿业与冶金

引用本文复制引用

李宝让,高慧,张乃强,徐鸿..煅烧制度对Lu2Ti2O7粉体生长形貌的影响[J].人工晶体学报,2012,41(1):146-151,6.

基金项目

教育部青年基金(09MG29) (09MG29)

人工晶体学报

OA北大核心CSCDCSTPCD

1000-985X

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