中国药业2012,Vol.21Issue(7):20-22,3.
赤芍配方颗粒质量标准研究
Study on Quality Standard of Chishao Dispensing Granule
张秀环 1胡昌江 1戴德蓉 1冯健1
作者信息
- 1. 四川新绿色药业科技发展股份有限公司药物研究所,四川成都,611930
- 折叠
摘要
Abstract
Objective To establish the quality standard for Chishao Dispensing Granules. Methods The TLC was used to identify Chishao Dispensing Granule; the content of the main active constituent paeoniflorin in the granule was determined by HPLC. Results The characteristic spots in TLC identification were clear and strong specific. There was a good linear relationship between the peak area and quantity of paeoniflorin at the range of 0. 243-4. 850 μg, r =0. 999 97, and the average recovery rate was 102. 11% , RSD was 1. 52% (n = 6). Conclusions The method is practicable and repeatable.It provides a sensitive and reliable analytical approach for the quality evaluation of Chishao Dispensing Granule.关键词
赤芍配方颗粒/薄层色谱法/高效液相色谱法/质量标准Key words
Chishao Dispensing Granule/TLC/HPLC/quality standard分类
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张秀环,胡昌江,戴德蓉,冯健..赤芍配方颗粒质量标准研究[J].中国药业,2012,21(7):20-22,3.