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Bi_2MoO_6空心球的水热沉淀法制备及其光催化性能

安丽 雅菁 刘志锋 鄂磊 刘成成 王丽婧

材料科学与工程学报2012,Vol.30Issue(2):283-286,226,5.
材料科学与工程学报2012,Vol.30Issue(2):283-286,226,5.

Bi_2MoO_6空心球的水热沉淀法制备及其光催化性能

Preparation and Properties of Bi_2MoO_6 Hollow Spheres by Hydrothermal Precipitation Method

安丽 1雅菁 1刘志锋 1鄂磊 1刘成成 1王丽婧1

作者信息

  • 1. 天津城市建设学院材料科学与工程系,天津300384
  • 折叠

摘要

Abstract

Colloidal carbon spheres with a hydrophilic surface were synthesized using glucose as a precursor by hydrothermal method.Carbon/Bi2MoO6 hollow spheres were successfully prepared by employing colloidal carbon spheres as template in subsection hydrothermal precipitation method.scanning electron microscopy(SEM),X-ray diffractometry(XRD),Fourier transform infrared(FT-IR) spectroscopy and Brumauer-Emmett-Tller(BET)were applied to characterize the morphology and structure of the as-prepared colloidal carbon spheres and Bi2MoO6 hollow spheres.The formation mechanism and reaction process of Bi2MoO6 hollow spheres were proposed.The photocatalytic activity of Bi2MoO6 hollow spheres has been tested on decomposable methylene blue under clarinet lamp.The results showed that Bi2MoO6 hollow spheres were composed of nanocrystals,the thickness was about 30~50nm,and the mean diameter was up to 0.6~0.8μm.The BET surface area of Bi2MoO6 hollow spheres and powders were about 11.315m2/g and 3.378m2/g,respectively.When the initial concentration of methylene blue(MB) was 10mg/L,the degradation rate of MB reached to 91.95% under clarinet lamp for 2.5 h by Bi2MoO6 hollow spheres.

关键词

胶体碳球模板/Bi2MoO6/空心球/光催化

Key words

colloidal carbon spheres template/Bi2MoO6/hollow spheres/photocatalytic

分类

化学化工

引用本文复制引用

安丽,雅菁,刘志锋,鄂磊,刘成成,王丽婧..Bi_2MoO_6空心球的水热沉淀法制备及其光催化性能[J].材料科学与工程学报,2012,30(2):283-286,226,5.

基金项目

天津市自然科学基金资助项目 ()

材料科学与工程学报

OA北大核心CSCDCSTPCD

1673-2812

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