硅酸盐学报2012，Vol.40Issue(2)：266-270,5.
溶胶-凝胶法制备纳米羟基磷灰石粉体
Synthesis of Nano-Sized Hydroxyapatite by Powder Sol-Gels Method
徐晓虹 1吴建锋 1华全 1倪扬 1闫宇嵩 1沈薇薇1
作者信息
- 1. 武汉理工大学材料科学与工程学院,武汉430070
- 折叠
摘要
Abstract
The nano-sized hydroxyapatite （HAP） powder was synthesized with Ca（NO3）2＂4H20 and P205 by a sol-gels process. The effects of pH value of solvent, reaction temperature and heated temperature on the crystallinity and morphology of nano-sized HAP were investigated by thermogravimetric/differential thermal analyzer, X-ray diffraction, transmission electron microscopy and Fourier transform infrared spectroscopy, respectively. The nano-particles of HAP with a higher crystallinity and a good disparity could be controlled via the adjustment of the process parameters such as reaction temperature, pH value of solution and heat treatment tem- perature. The results show that the nano-particles of HAP containing CO32- with the good crystallinity and the particle sizes of 40-50 nm could be obtained at the reaction temperature of 30 ℃, the pH value of 8 and the heat treatment temperature of 600 ℃.关键词
溶胶-凝胶法：羟基磷灰石/纳米粉体/制备工艺/显微结构Key words
sol-gels method/hydroxyapatite/nano-powder/process/microstructure分类
医药卫生引用本文复制引用
徐晓虹,吴建锋,华全,倪扬,闫宇嵩,沈薇薇..溶胶-凝胶法制备纳米羟基磷灰石粉体[J].硅酸盐学报,2012,40(2):266-270,5.
