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月桂酸插层改性Ni/Al-NO3-LDHs及其对摩擦性能的影响

赵栋 白志民

硅酸盐学报2012,Vol.40Issue(5):769-775,7.
硅酸盐学报2012,Vol.40Issue(5):769-775,7.

月桂酸插层改性Ni/Al-NO3-LDHs及其对摩擦性能的影响

Ni/Al-NO3-LDHs Intercalated with Dodecanoic Acid and its Tribological Characteristics

赵栋 1白志民1

作者信息

  • 1. 中国地质大学材料科学与工程学院,北京100083
  • 折叠

摘要

Abstract

The nickel aluminum layered double hydroxides(Ni/Al-NO3-LDHs) intercalated with dodecanoic acids were prepared via coprecipitation by an anion exchange method.The obtained compounds were characterized by X-ray diffraction,Fourier transform infrared spectroscopy,thermogravimetry-differential scanning calorimetry,scanning electron microscopy and specific surface area analysis,respectively.The tribological performance in the base oil was investigated by a four-ball wear machine and a gear testing machine.The results indicate that the shape of the crystal obtained before the intercalation appears hexagonal flake with the crystal size of 40 nm and the specific surface area of 96.57 m2/g.After the intercalation,the channel height of Ni/Al-NO3-LDHs increased,but the specific surface area decreased.The Ni/Al-NO3-LDHs and its products intercalated with dodecanoic acid could reduce the friction coefficient,wear scar diameter,lubrication medium temperature and drive motor power as well.

关键词

镍铝类水滑石/月桂酸/插层/摩擦性能

Key words

nickel aluminum layered double hydroxides/dodecanoic acid/intercalation/tribological performance

分类

化学化工

引用本文复制引用

赵栋,白志民..月桂酸插层改性Ni/Al-NO3-LDHs及其对摩擦性能的影响[J].硅酸盐学报,2012,40(5):769-775,7.

基金项目

国家自然科学基金(51044011)资助项目 ()

硅酸盐学报

OA北大核心CSCDCSTPCD

0454-5648

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