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啤酒中胺类物质的系统分析

郑金珠 刘翻 孙元社 唐涛 张维冰 李彤

生命科学仪器2012,Vol.10Issue(1):23-26,4.
生命科学仪器2012,Vol.10Issue(1):23-26,4.

啤酒中胺类物质的系统分析

System analysis of amines in beer

郑金珠 1刘翻 2孙元社 3唐涛 3张维冰 2李彤3

作者信息

  • 1. 齐齐哈尔大学,黑龙江齐齐哈尔161000
  • 2. 上海市功能性材料化学重点实验室,华东理工大学,上海200237
  • 3. 大连依利特分析仪器有限公司,辽宁大连116023/辽宁大连依利特分析仪器工程技术研究中心,辽宁大连116023
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摘要

Abstract

Many amine compounds are exist in Beer. Whose taste and quality are closely related to the content and the kind of the amine compounds. A method for trace amine compounds analysis in beer was developed in this paper. The amine compounds withNH2 and NH in beer were analyzed by HPLC separation and LIFD determination, using FITC as derivative regent. Then the nitrosamines in beer were quantitative analyzed by lowtemperature vacuum distillation com bined with GCFID. Further more, various kinds of beer on sell were analyzed. Using the developed method, the result indicated that there existed some differences of amine compounds among different brands and different series of beer. Setting the integral threshold at lmv, the largest number of HPLC peaks is 53 and the least number is 38. In the chromato grams of beer samples, Analyze the content of nitrosamines in three kinds of beer and trace nitrosamines have been de tected in two kinds of them. The method has a high sensitivity, good stability and is easily operated. It can be used for de tection of quality of beer and fake and shoddy products and is valuable significance to control the content of carcinogenic amine compounds. It is very important for the health of people. The method is also suitable for amine compounds analysis in other beverage and food.

关键词

胺类物质/啤酒/HPLC-LIFD/GC-FID

Key words

Amines/Beer/HPLC-LIFD/GC-FID

分类

化学化工

引用本文复制引用

郑金珠,刘翻,孙元社,唐涛,张维冰,李彤..啤酒中胺类物质的系统分析[J].生命科学仪器,2012,10(1):23-26,4.

基金项目

国家重点基础研究发展规划(973)项目 ()

食品科学与技术国家重点实验室2010年度开放基金 ()

国家自然科学基金 ()

生命科学仪器

1671-7929

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