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氨基硅烷化磁性纳米粒子的制备与表征

顾银君 王秀玲 陈恭 赵勤 刘勇健 张利杰

苏州科技学院学报:自然科学版2012,Vol.29Issue(1):42-46,5.
苏州科技学院学报:自然科学版2012,Vol.29Issue(1):42-46,5.

氨基硅烷化磁性纳米粒子的制备与表征

Synthesis and characterization of magnetic nanoparticles modified by 3-aminopropyltriethoxy-silane

顾银君 1王秀玲 1陈恭 1赵勤 2刘勇健 1张利杰1

作者信息

  • 1. 苏州科技学院化学与生物工程学院.江苏苏州215009
  • 2. 苏州大学材料与化学化工学部,江苏苏州215123
  • 折叠

摘要

Abstract

Superparamagnetic Fe304 nanoparticles were first synthesized by hydrothermal coprecipitation of ferric and ferrous ions, followed by the modification of their surfaces with 3-aminopropyhriethoxy-silane (APTES). The structure and properties of as-synthesized nanoparticles were characterized by FTIR,TEM,TGA,and vibrating sample magnetometer (VSM). The results indicate that nanoparticles are coated successfully by APTES. The coat- ing layer gradually becomes complete and thicker with the addition of APTES. It also shows that the magnetic properties of magnetic nanocomposites are enhanced with the addition of APTES within certain degree. Beyond this, the magnetic performance decreases.

关键词

磁性纳米粒子/氨基化/表面修饰/制备/表征

Key words

magnetic nanoparticles/amino-functionalization/surface modification/synthesis/characterization

分类

化学

引用本文复制引用

顾银君,王秀玲,陈恭,赵勤,刘勇健,张利杰..氨基硅烷化磁性纳米粒子的制备与表征[J].苏州科技学院学报:自然科学版,2012,29(1):42-46,5.

基金项目

国家自然科学基金资助项目 ()

苏州科技学院研究生科研创新计划项目 ()

苏州科技学院学报:自然科学版

2096-3289

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