印染助剂2012，Vol.29Issue(4)：16-17,2.
二甲氨基丙基丙烯酰胺改性含氢硅油的合成
Synthesis of N,N-dimethylaminopropylacrylamide modified hydrogen silicone oil
摘要
Abstract
Amino modified silicone was prepared by the hydrosilation using N,N-dimethylaminopro-pylacrylamide and hydrogen silicone oil as materials, chloroplatinic acid-isopropanol as catalyst, and toluene as solvent. The dosage of toluene was 1.5 times of the sum mass of hydrogen silicone oil and N,N-dimethylami-nopropylacrylamide, the mass of inhibitor was 0.5% on the mass of monomer, the mole ration of hydrogen silicone oil and monomer was 1:1.1, the catalyst amount was 50x10-6 on the mass of reactant, and the hydrosilation was carried out at 120 ℃. The structure of the polymer was analyzed by IR. The result indicated that the amino group introduced into the side chain of hydrogen silicone oil, and the amino modified silicone oil was prepared.关键词
二甲氨基丙基丙烯酰胺/含氢硅油/硅氢加成反应/氨基改性硅油Key words
N,N-dimethylaminopropylacrylamide/ hydrogen silicone oil/ hydrosilation/ amino modified silicone oil分类
化学化工引用本文复制引用
赵欣,朱文英,刘苏..二甲氨基丙基丙烯酰胺改性含氢硅油的合成[J].印染助剂,2012,29(4):16-17,2.基金项目
黑龙江省振兴东北老工业基地项目"高档亚麻与色织而料编号:1151gzd22" （）
